( GC system )
model : 7890B
1. System Capabilites
1) Supports simultaneously
- two inlets
- Three detectors (third detector as
TCD or ECD)
2) Column Oven
- Diamensions : 28 * 31 *
16 cm
- Operating temperature range :
+4¡É to 450¡É
( GC-MASS system)
model : 5977A MSD
1. Mass Selective Detector
1) EI Source :
Standard Inert or high sensitivity Extractor
2) CI
Source : PCI, NCI, and acquisition
3) Ion source
temperature : 150 - 350¡É
4) Quadrupole
temperature : 106 - 200¡É
5) Mass filter
: Monolithic hyperbolic quadrupole
6) Mass range
: 1.6 - 1050 u
7) Mass axis
stability : Better than 0.10u / 48h
8) Detector :
Triple-Axis Detector with long life EM
( Multi-Shot Pyrolyzer )
model : PY-3030D
1. Performance guaranteed (detector : MS & FID)
1)
Reproducibility of pyrograms
- In
flash pyrolysis of PS (25 ¥ìg) at 550¨¬C (Eco cup LF used), the relative standard
deviation (RSD) of the peak area ratio of styrene trimer (SSS) and methyl
stearate(Me-Ste): ¡Â2% (Eco cup LF)
2)
Reproducibility of EGA thermograms
- RSD
of the peak top temperature of PS: ¡Â0.3%
2. Furnace and sampling unit
1) Pyrolyzer
furnace : Cylindrical ceramic heater
-
Temperature control range/Stability : Room temperature + 10¨¬C up to 1050¨¬C (1¨¬C
step) / ¡¾0.1¨¬C
-
Cooling system : Forced air cooling by nitrogen or compressed air
-
Cooling time (pressure: 500kPa) : Within 10 min (800¨¬C down to 50¨¬C when ITF in
auto mode)
2) Interface
(ITF) (Cartridge heater)
-
Temperature/Stability : 40 up to450¨¬C (1¨¬C step) / ¡¾0.1¨¬C
3) Sampler
-
Double-shot sampler and Liquid sampler
4) Deactivated
sample cup
- Eco
cup SF(50 ¥ìL) and LF (80 ¥ìL)
3. Temperature controller
1) Overheat
protection temperature : PY: 1100¨¬C, ITF: 500¨¬C
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